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本发明提供了一种制备4-羰基环己基甲酸乙酯的方法,将二水合钨酸钠、丙二酸混合搅拌,再加入双氧水制得氧化剂,向上述氧化剂中加入反应物4-羟基环己基甲酸乙酯和溶剂乙腈,反应后制得4-羰基环己基甲酸乙酯。本发明中氧化剂双氧水
The present invention provides a method for preparing ethyl 4-carbonyl cyclohexyl carboxylate, mixing and stirring sodium tungstate dihydrate and malonic acid, adding hydrogen peroxide to obtain an oxidant, adding the reactant 4-hydroxycyclohexyl Ethyl formate and solvent acetonitrile to give ethyl 4-carbonyl cyclohexylcarboxylate after reaction. In the present invention, the oxidant hydrogen peroxide