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叔十二硫醇主要用作橡胶、树脂及纤维生产中控制相对分子质量的链调节剂。文中介绍了多种合成叔十二硫醇的方法,并以三氯化铝作催化剂,由十二烯和硫化氢合成了叔十二硫醇,考察了影响收率的因素,叔十二硫醇收率达80%。
Tert-dodecanethiol mainly used as rubber, resin and fiber production chain regulator to control the relative molecular mass. In this paper, a variety of synthetic tert-dodecanethiol methods are introduced. Aluminum trichloride is used as a catalyst to synthesize t-dodecyl mercaptan from dodecene and hydrogen sulfide. The factors influencing the yield are investigated. Alcohol yield of 80%.