【摘 要】
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The binuclear complex [Sm2(C12H8N2)2(C6H5COO)6] has been prepared and structurally analyzed by single crystal X-ray diffraction. The complex crystallizes in the
【机 构】
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Department of Chemistry,Jilin University
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The binuclear complex [Sm2(C12H8N2)2(C6H5COO)6] has been prepared and structurally analyzed by single crystal X-ray diffraction. The complex crystallizes in the triclinic system, space group P(1), with a=10.833(2), b=11.937(2), c=12.448(3)(A), α= 104.97(3), β= 93.63(3), γ= 113.27(3)°, V=1403.5(A)3, Dc=1.64g/cm3, μ=21.42cm-1, F(000)=690, Z=1, final R=0.037, Rw=0.077 for 4855 observed reflections [I>2σ(I)] and 5703 independent reflections. In the molecule, each Sm atom is coordinated by seven O atoms and two N atoms forming an irregular coordination polyhedron.
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