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介绍了间二氟甲氧基硝基苯毛细管气相色谱测定方法，色谱条件为：程序升温，内标物为邻苯二甲酸二甲酯。间二氟甲氧基硝基苯的浓度在０． ８～８．０ ｍｇ／ｍＬ的范围内，样品有良好的线性关系，ｒ≥０．９９９７。
The method for the determination of m-difluoromethoxynitrobenzene by capillary gas chromatography was introduced. The chromatographic conditions were as follows: the temperature was raised and the internal standard was dimethyl phthalate. The concentration of m-difluoromethoxynitrobenzene is zero. 8 ~ 8.0 mg / mL range, the sample has a good linear relationship, r ≥ 0.997.