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土壤或玉米植株样品用V(甲醇)∶V(乙腈)=1∶1提取,提取液用石油醚净化后,浓缩液过C18小柱净化,最后用Nova-PakC18柱进行HPLC分析。回收率:氰草津为82.4%~99.8%,莠去津为85.6%~102.3%,西草净为89.1%~108.4%。
Soil or corn plant samples were extracted with V (methanol): V (acetonitrile) = 1: 1. The extract was purified with petroleum ether and the concentrate was purified on a C18 cartridge and finally analyzed by Nova-Pak C18 column for HPLC. The recoveries of cyanazine: 82.4% ~ 99.8%, atrazine: 85.6% ~ 102.3%, and simethicone: 89.1% ~ 108.4%.